ADVANCED PRODUCTION TECHNOLOGY OF HIGH PURITY ARABINOGALACTAN

  • Елена (Elena) Николаевна (Nikolaevna) Медведева (Medvedeva) A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences Email: woodemed@irioch.irk.ru
  • Юрий (Yurij) Алексеевич (Аlekseevich) Малков (Malkov) A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences Email: malkov@irioch.irk.ru
  • Василий (Vasilij) Анатольевич (Аnatol'evich) Бабкин (Babkin) A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences Email: babkin@irioch.irk.ru
Keywords: arabinogalactan, technology, larch biomass, ultrafiltration, diafiltration, membranes

Abstract

The technology of larch wood arabinogalactan production, combined with the preparation of dihydroquercetin, has been developed. The improved process includes the following steps: extraction of larch raw material with hot water (80–90 °C) after extraction of dihydroquercetin from it; purification of the obtained extract from high-molecular impurities by ultrafiltration using a hydrophobic membrane; concentration and additional purification of the extract from low molecular weight phenolic impurities by diafiltration using a hydrophilic membrane; spray drying of the concentrate. The concentrate drying parameters are optimized. The improved technology makes it possible to obtain a product with a main substance content ≥98%, to exclude the use of imported reagents – flocculants, and, therefore, the expenses of separation from clarified extract cake and its utilization are eliminated. Undoubted advantages of the developed technology are the reduction of the purification time of the extract, as well as the ability to automate the process of AG production and realize it in a continuous mode, that increase the feasibility and economic efficiency of the process, as well as to increase the exploitation time of the hydrophilic membrane, and to reduce energy costs.

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Author Biographies

Елена (Elena) Николаевна (Nikolaevna) Медведева (Medvedeva), A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences
кандидат химических наук, старший научный сотрудник
Юрий (Yurij) Алексеевич (Аlekseevich) Малков (Malkov), A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences
кандидат технических наук, главный специалист
Василий (Vasilij) Анатольевич (Аnatol'evich) Бабкин (Babkin), A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences
доктор химических наук, профессор, заведующий лабораторией химии древесины

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Published
2018-01-15
How to Cite
1. Медведева (Medvedeva)Е. (Elena) Н. (Nikolaevna), Малков (Malkov)Ю. (Yurij) А. (Аlekseevich), Бабкин (Babkin)В. (Vasilij) А. (Аnatol’evich) ADVANCED PRODUCTION TECHNOLOGY OF HIGH PURITY ARABINOGALACTAN // chemistry of plant raw material, 2018. № 2. P. 183-189. URL: http://journal.asu.ru/cw/article/view/3435.
Section
Technology