THE COMPONENT COMPOSITION OF THE RHIZOMES OF THE CIRSIUM HELENIOIDES (L.) HILL
UDC 543.544:615.582.9
Abstract
The biologically active substances of water-alcohol extraction from the rhizomes of wild elderberry (Cirsium helenioides (L.) Hill) were studied in the work. Samples of raw materials were harvested on the territory of the Kemerovo region ‒ Kuzbass. The study was carried out using a complex of chromatographic (low pressure column chromatography, HPLC, GC-MS, TLC) and spectral (electron spectroscopy, IR–FT) analysis methods. Low-pressure chromatography was performed using sephadex LH-20 modified with vancomycin as a sorbent. The use of this sorbent made it possible to carry out the preparative accumulation of key components, as well as minor components. Thus, the isomers p - coumaric acid and caffeic acid were isolated into separate fractions. Phytosterols campesterol and stigmasterol were isolated and preparatively accumulated for the first time. It has been established that water-alcohol extraction from the underground part of the plant contains simple phenylpropanoids: p-coumaric, caffeic, ferulic acids. The presence of monoterpene borneol is shown for the plant. The content of carbohydrate components was determined, which are represented by monosaccharides: glucopyranose, fructose, β-D-(+)-xylopyranose. The presence of the following polyatomic alcohols was noted: meso-erythritol, ribitol.
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