COPMONENT COMPOSITION OF ROOT IN TWO SPECIES OPLOPANAX (ARALIACEAE)

UDC 633.8:54.061:543.544.3

  • Yelizaveta Sergeyevna Zhestovskaya FSUE Scientific Center "Signal" Email: Zhestovskayae@gmail.com
  • Sergey Valer'yevich Vasilevskiy FSUE Scientific Center "Signal" Email: vasilevs73@yandex.ru
  • Aleksey Vadimovich Aksenov FSUE Scientific Center "Signal" Email: aksenov_av@list.ru
  • Viktor Fedorovich Taranchenko FSUE Scientific Center "Signal" Email: victaran@rambler.ru
  • Andrey Nikolayevich Stavrianidi Lomonosov Moscow State University Email: stavrianidi.andrey@analyt.chem.msu.ru
  • Oleg Alekseyevich Shpigun Lomonosov Moscow State University Email: shpigun@analyt.chem.msu.ru
Keywords: Oplopanax horridus, Oplopanax elatus, gas chromatography, mass-spectrometry

Abstract

The qualitative and quantitative composition of two species of Oplopanax root was studied by gas chromatography with mass spectrometric detection. Extraction of components from the investigated objects was carried out by extraction of dry ground raw material with 70% ethanol. For the analysis of polar compounds, the extracts were further derivatized to give the corresponding trimethylsilyl derivatives. Identification of components was carried out using commercial (NIST17, Wiley14) and own custom mass-spectrometer libraries. The percentage of components found was calculated using the areas of the corresponding chromatographic peaks. Found in these samples were 130 compounds of various classes: terpenes and their derivatives, alcohols, aldehydes, polyyns, polyenes, various acids and their derivatives, phenols, sterols, lignans, vitamins, nucleosides, glycosides and sugars. It has been established that the qualitative and quantitative composition of root extracts varies even within the same species. The presence of 26 compounds common to the two species of Oplopanax, including 12 acids, 3 polyyns, 6 terpenes and one representative each from the class polyenes, aldehydes, lignans, glycosides and sterols, was revealed. As a result of the comparative analysis, it was established that 4 compounds from the class of polyyns (falcarindiol acetate, oplopanediol acetate, oplopantriol A and oplopantriol B) are found only in the roots of O. horridus.

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Author Biographies

Yelizaveta Sergeyevna Zhestovskaya, FSUE Scientific Center "Signal"

научный сотрудник

Sergey Valer'yevich Vasilevskiy, FSUE Scientific Center "Signal"

кандидат химических наук, доцент, заведующий лабораторией

Aleksey Vadimovich Aksenov, FSUE Scientific Center "Signal"

кандидат технических наук, доцент, заведующий лабораторией

Viktor Fedorovich Taranchenko, FSUE Scientific Center "Signal"

кандидат химических наук, доцент, начальник отдела

Andrey Nikolayevich Stavrianidi, Lomonosov Moscow State University

кандидат химических наук, доцент кафедры аналитической химии

Oleg Alekseyevich Shpigun, Lomonosov Moscow State University

доктор химических наук, член-корреспондент РАН, профессор кафедры аналитической химии

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Published
2019-12-27
How to Cite
1. Zhestovskaya Y. S., Vasilevskiy S. V., Aksenov A. V., Taranchenko V. F., Stavrianidi A. N., Shpigun O. A. COPMONENT COMPOSITION OF ROOT IN TWO SPECIES OPLOPANAX (ARALIACEAE) // chemistry of plant raw material, 2019. № 4. P. 233-242. URL: http://journal.asu.ru/cw/article/view/5219.
Section
Low-molecular weight compounds